HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylacetate heptane → HCID 53312108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylacetate heptane | HCID 21899848 | — |
| Reactant | 4-(2,5-dichloro-phenoxy)-N-(2-dimethylamino-pyridin-3-yl)-nicotinamide | HCID 67320131 | — |
| Product | HCID 53312108 | HCID 53312108 | — |
Reaction Steps
The title compound was prepared in analogy to Example 12, from 4-(2,5-dichloro-phenoxy)-N-(2-dimethylamino-pyridin-3-yl)-nicotinamide and using a gradient of n-heptane:ethyl acetate (100:0 to 0:100) for the chromatographic purification. Colorless oil (67%). MS (ESI): m/z=417.088 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08420647B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-58350c731dac4952a5a2b84f1650324c |
| Source note | uspto-grants-2013_04 |