Methanol → Methyl 5-phenylpentanoate

HRID 1967081노트

반응식

[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][C:11]([OH:13])=[O:12])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:14]O>>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][C:11]([O:13][CH3:14])=[O:12])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

반응물 2

HCID 887Methanol

HCID 16757Benzenepentanoic acid

생성물 1

HCID 262942Methyl 5-phenylpentanoate

실험 절차

5-Phenylpentanoic acid (10.0 g) was dissolved in 250 mL of methanol and sparged with hydrogen chloride gas at room temperature for 15 minutes. The solvent was then removed under vacuum. Methyl 5-phenylpentanoate obtained was used in the next step without further purification.

후처리

customsparged with hydrogen chloride gas at room temperature for 15 minutes
customThe solvent was then removed under vacuum

출처 및 근거

ORD 기록: ord-eb05df898bc047a292c730ce5cd1d879
출처 데이터셋: uspto-grants-2013_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08420698B2

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