Iodoethane → HCID 66872688, compound

Participants

Reaction Steps

The compound (30 mg) obtained in Example 151 was dissolved in DMF (0.50 mL), then potassium carbonate (30 mg) and iodoethane (0.030 mL) were added thereto in that order, and stirred at room temperature for 18 hours. This was purified through reversed-phase HPLC (0.1% TFA acetonitrile/H2O=from 10% to 95%, gradient) to give the entitled compound (25 mg, 78%) as a colorless solid.

Provenance & Evidence