反应详情

A solution of N-[2,6-dimethyl-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)-phenyl]-2,6-dimethoxy-3-nitrobenzamide (200 mg, 0.4 mmol) (see Example I3) in ethanol (8 ml) charged with Pd/C 10% (64 mg, 0.06 mmol) was stirred under a hydrogen atmosphere for 16 hours. After filtration the mixture was concentrated. The residue was used without further purification.

1. filtrationAfter filtration the mixture
2. concentrationwas concentrated
3. customThe residue was used without further purification