Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Chloropyrazine-2-carbonitrile | HCID 292465 | — |
| Reactant | HCID 178418558 | HCID 178418558 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178510581 | HCID 178510581 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 by using 1,3,4-thiadiazole-2,5-dithiol (945 mg, 6.05 mmol), NaH (60% dispersion in mineral oil, 264 mg, 6.60 mmol), and 3-chloropyrazine-2-carbonitrile (840 mg, 6.00 mmol) in DMF and benzene (10 ml, 1/1) by stirring at 50° C. under nitrogen atmosphere for 4 hr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08426358B2 |
|---|
| Source dataset | uspto-grants-2013_04 |
|---|
| ORD ID | ord-a05cb52aa21a4618a55ce190abd84a07 |
|---|
| Source note | uspto-grants-2013_04 |
|---|
