Water → HCID 25111366, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of (E)-S-4-(3,5-dimethoxystyryl)phenyl dimethylcarbamothioate (50 mg, 0.14 mM) in ethyl ether (10 mL) was added LiAlH4 (6 mg, 0.14 mM) at 0° C. The reaction mixture was stirred at 65° C. for 3 h. The mixture was poured into water (10 mL) and a solution of 1M HCL (10 mL). The crude mixture was purified by column chromatography eluting with hexanes:ethyl acetate (4:1) and gave ARS27.

Provenance & Evidence