rel-(1R,2R,3S,4S)-3-Aminobicyclo[2.2.1]hept-5-ene-2-carboxamide → HCID 13724496, compound

Participants

Reaction Steps

A solution of (+/−)-(1S,2S,3R,4R)-3-aminobicyclo[2.2.1]hept-5-ene-2-carboxamide (707 mg, 4.65 mmol) in methanol (23 ml) was evacuated and purged with nitrogen and treated with palladium on carbon (74.2 mg, 0.070 mmol). The resulting suspension was evacuated and purged with a hydrogen balloon and stirred under the hydrogen overnight. The mixture was filtered through celite, washed with methanol, and dried to afford the title compound.

Provenance & Evidence