HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 67144534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Methyl 4-fluorosalicylate | HCID 2775386 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67144534 | HCID 67144534 | — |
Reaction Steps
Methyl 4-fluoro-2-hydroxybenzoate (2.00 g), benzyl bromide (1.54 mL), and cesium carbonate (4.60 g) in N,N-dimethylformamide (50 mL) were stirred in for 24 hours. The reaction was taken up in ether and washed 3× with 1M NaOH solution and with brine, then concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426422B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-5adec329bfb449b5adf39f4385ee11a0 |
| Source note | uspto-grants-2013_04 |