HRID1968770

反应详情

EQUATION

反应方程式

HRID 1968770 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3-(5-benzoyl-2-nitro-benzylamino)-N-cyclohexyl-N-methyl-propionamide (9 g, 0.02 mol), 10% palladium on carbon (2 g), and thiophene solution (2 mL) in MeOH (250 mL) was hydrogenated until 3 equivalents of hydrogen were consumed. The reaction mixture was filtered through Dicalite, and the filtrate was concentrated to yield a residue.

WORKUP

后处理

  1. customwere consumed
  2. filtrationThe reaction mixture was filtered through Dicalite
  3. concentrationthe filtrate was concentrated
  4. customto yield a residue