HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamyl nitrate → HCID 66995397, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamyl nitrate | HCID 10985 | — |
| Reactant | HCID 66995399 | HCID 66995399 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66995397 | HCID 66995397 | — |
Reaction Steps
3-Methylbutyl nitrate was dissolved in a tetrahydrofuran solution of ethyl 4-amino-3-(3-cyano-4-methoxyphenyl)isothiazole-5-carboxylate, followed by heating under reflux for 5 hours to obtain ethyl 3-(3-cyano-4-methoxyphenyl)isothiazole-5-carboxylate. AP: 311.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426453B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-2f5db3f1722e44b3a7d94af05ebad0c1 |
| Source note | uspto-grants-2013_04 |