HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (4-mercapto-2-methylphenoxy)acetate → HCID 57791906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (4-mercapto-2-methylphenoxy)acetate | HCID 16641178 | — |
| Reactant | 2-(3,5-Dibromophenoxy)-3-(trifluoromethyl)pyridine | HCID 66524309 | — |
| Product | HCID 57791906 | HCID 57791906 | — |
Reaction Steps
2-(3,5-Dibromo-phenoxy)-3-trifluoromethyl-pyridine (2.05 g; 5.17 mmol) and (4-Mercapto-2-methyl-phenoxy)-acetic acid ethyl ester (0.9 g; 4.0 mmol) was condensed to give the title product applying the procedure described for {4-[3-Bromo-5-cyclopentylmethoxy-phenylsulfanyl)-2-methyl-phenoxy]-acetic acid ethyl ester. The crude product was purified by flash chromatography (heptane→ethyl acetate:heptane 2:9). Yield 1.26 g (58%). HPLC-MS: m/z: 544.3 (M+2); Rt: 2.77 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426473B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-ae73b7ad8eb34697bebe9c05fec370f1 |
| Source note | uspto-grants-2013_04 |