2-Amino-4-phenylphenol → HCID 68741696, compound

HRID 1969296Notes

Reaction equation

HRID 1969296 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH:5]=[CH:6][C:7]=1[OH:8].[F:15][C:16]([F:31])([F:30])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[C:23]1[O:27][C:26]([CH:28]=O)=[CH:25][CH:24]=1>>[F:31][C:16]([F:15])([F:30])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[C:23]1[O:27][C:26]([CH:28]=[N:1][C:2]2[CH:3]=[C:4]([C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=3)[CH:5]=[CH:6][C:7]=2[OH:8])=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 145622-Amino-4-phenylphenolHCID 6882805-[2-(trifluoromethyl)phenyl]furan-2-carbaldehyde

Product 1

HCID 68741696HCID 68741696, compound

Procedure

Using 3-aminobiphenyl-4-ol and 5-(2-(trifluoromethyl)phenyl)furan-2-carbaldehyde, 1.64 g of 3-{[5-(2-(trifluoromethyl)phenyl)furan-2-yl]methyleneamino}biphenyl-4-ol was obtained as an orange powder (yield 34%).

Sources & evidence

ORD record
ord-454747af42eb419d9df90b2e66643664
Source dataset
uspto-grants-2013_04
Patent number
US08426540B2

Reaction notes

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