3-Chlorobenzenesulphonyl chloride → HCID 86627491, compound

Participants

Reaction Steps

This compound is prepared according to synthesis 37, from 60 mg (0.22 mmol) of 8-amino-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate (synthesis 64) and 34 μL (0.24 mmol) of 3-chloro-benzenesulfonyl chloride. After recrystallization from methanol then trituration in hot methanol, 27 mg (27%) of 8-(3-chloro-benzenesulfonylamino)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate is obtained in the form of a white solid.

Provenance & Evidence