3-Methoxybenzenesulfonyl chloride → HCID 86627500, compound

Participants

Reaction Steps

This compound is prepared according to synthesis 43, from 60 mg (0.20 mmol) of 8-amino-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate hydrochloride (synthesis 64) and 30 μL (0.21 mmol) of 3-methoxy-benzenesulfonyl chloride. After recrystallization from methanol then trituration in hot methanol, 21 mg (25%) of 8-(3-methoxy-benzenesulfonylamino)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-ethyl carboxylate is obtained in the form of a beige solid.

Provenance & Evidence