HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanemethylamine → HCID 15605165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanemethylamine | HCID 76688 | — |
| Reactant | 4-oxo-3H,4H,5H-pyrrolo[2,3-c]quinoline-1-carboxylic acid | HCID 12065084 | — |
| Product | HCID 15605165 | HCID 15605165 | 8% |
Reaction Steps
This compound is prepared according to synthesis 79 from 75 mg (0.33 mmol) of 4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxylic acid (synthesis 75) and 47 μL (0.36 mmol) of C-cyclohexyl-methylamine. After recrystallization from methanol, 8 mg (8%) of N-(cyclohexylmethyl)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxamide is obtained in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-b80aeaaeb7e046a384fcf243acab30b7 |
| Source note | uspto-grants-2013_04 |