HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N-(phenyl)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 4-oxo-3H,4H,5H-pyrrolo[2,3-c]quinoline-1-carboxylic acid | HCID 12065084 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-(phenyl)-4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxamide | HCID 15605285 | 45% |
Reaction Steps
This compound is prepared according to synthesis 79 from 75 mg (0.33 mmol) of 4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxylic acid (synthesis 75) and 33 μL (0.36 mmol) of aniline. After trituration in diethyl ether, 45 mg (45%) of N-(phenyl)-4-oxo-4,5-dihydro-3H -pyrrolo[2,3-c]quinoline-1-carboxamide is obtained in the form of a light brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-ba63e89efb46415081a5c8b77be694ff |
| Source note | uspto-grants-2013_04 |