HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86627562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-oxo-3H,4H,5H-pyrrolo[2,3-c]quinoline-1-carboxylic acid | HCID 12065084 | — |
| Reactant | HCID 86627563 | HCID 86627563 | — |
| Product | HCID 86627562 | HCID 86627562 | — |
Reaction Steps
4-Oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-cyclopentyl carboxylate was prepared according to method of esterification C from 194 mg (0.85 mmol) of 4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-carboxylic acid, 1.29 mL (12.75 mmol) of triethylamine and 1.99 g (8.5 mmol) of dicyclopentylsulfate to give, after precipitation in water, 250 mg (98%) of 4-oxo-4,5-dihydro-3H-pyrrolo[2,3-c]quinoline-1-cyclopentyl carboxylate in the form of a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08426437B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-8096631eced042ceb30f4125ab467016 |
| Source note | uspto-grants-2013_04 |