HRID1970465

反应详情

EQUATION

反应方程式

HRID 1970465 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 1.8 g 4-butoxycarbonylamino-piperidine-1-carboxylic acid benzyl ester in 60 ml EtOH were added 200 mg Pd/C (10%) and the suspension stirred under an atmosphere of hydrogen (1 bar) for 2 h. The reaction mixture was filtrated over a plug of Celite and washed with EtOH to give the product as colorless oil after evaporation of the solvent.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtrated over a plug of Celite
  2. washwashed with EtOH