HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178454901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Di-tert-butylchlorophosphine | HCID 139566 | — |
| Product | HCID 178454901 | HCID 178454901 | 100.2% |
Reaction Steps
To a flask were added 1.0 g of di(tert-butyl)chlorophosphine and 5 ml of dichloromethane under nitrogen. After slow addition of 0.25 g of water, the mixture was stirred at 22 C for 30 minutes and the solvent was removed leaving a solid. After purification by sublimation, 0.9 g of a white solid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431045B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-2b79d966d7c24a7c832a190a255a7e5d |
| Source note | uspto-grants-2013_04 |