HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 11978438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 3-Pyridinylboronic acid | HCID 2734378 | — |
| Reactant | 4-(8-Bromo-2,3-dihydro-2-oxo-1H-imidazo(4,5-c)quinolin-1-yl)-alpha,alpha-dimethylbenzeneacetonitrile | HCID 42609569 | — |
| Product | HCID 11978438 | HCID 11978438 | — |
Reaction Steps
The title compound is prepared in a similar manner as described in Example 1 by reacting 2-[4-(8-bromo-2-oxo-2,3-dihydro-imidazo[4,5-c]quinolin-1-yl)-phenyl]-2-methyl-propionitrile (Example 1h) with iodoethane (Fluka, Buchs, Switzerland) and using 3-pyridineboronic acid. ES-MS: 434 (M+H)+; analytical HPLC: tret=2.55 min (Grad 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431592B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-11e6f8095e314b59824f4eb6d974f900 |
| Source note | uspto-grants-2013_04 |