1H-1,2,4-Triazole → 351325-27-4

HRID 1971240Notes

Reaction equation

HRID 1971240 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-])=O)=[CH:4][C:3]=1[C:11]([F:14])([F:13])[F:12].[NH:15]1[CH:19]=[N:18][CH:17]=[N:16]1>>[N:15]1([C:2]2[CH:7]=[CH:6][C:5]([NH2:8])=[CH:4][C:3]=2[C:11]([F:14])([F:13])[F:12])[CH:19]=[N:18][CH:17]=[N:16]1

Participants

3

Reactant 2

HCID 92571H-1,2,4-TriazoleHCID 949542-Fluoro-5-nitrobenzotrifluoride

Product 1

HCID 47002925351325-27-4

Procedure

The title compound is obtained in a similar manner as Example 71a using 1-fluoro-4-nitro-2-trifluoromethyl-benzene (Aldrich, Buchs, Switzerland) and 1,2,4-triazole (Fluka, Buchs, Switzerland). Title compound: ES-MS: 229 (M+H)+; analytical HPLC: tret=4.14 minutes (Grad 2).

Sources & evidence

ORD record
ord-34a28e3dcb8b410481478a77707812b3
Source dataset
uspto-grants-2013_04
Patent number
US08431592B2

Reaction notes

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