HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972121Generated: October 30, 2026
Methyl chloroformate → HCID 58452968, compound
https://huagongshe.com/reaction/1972121
Participants
| Role | Name | HCID | Charge |
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| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 7122702 | HCID 7122702 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58452968 | HCID 58452968 | — |
Reaction Steps
To a solution (1S,7S)-1,7-dimethyl-9-nitro-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinoline (7), (115 mg, 0.31 mmol), in dichloromethane (15 mL) was added three equivalent of triethyl amine (0.129 mL, 0.93 mmol), followed by methyl chloroformate (0.031 mL, 0.406 mmol) under argon at 0° C. The reaction mixture was then stirred at room temperature for overnight. The mixture was quenched with water (30 mL). The residue was isolated in a typical aqueous workup and purified by MPLC (medium pressure liquid chromatography) using silica gel column with 10 to 15% EtOAc:Hexane to give methyl (1S,7S)-1,7-dimethyl-1,7-diphenyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinolin-9-ylcarbamate (829), (69 mg 52%). 1H NMR (300 MHz, Acetone-d6) ppm 1.72 (s, 6H) 1.89-2.03 (m, 2H) 2.17-2.30 (m, 2H) 2.73-2.88 (m, 2H) 2.92-3.03 (m, 2H) 3.56 (s, 3H) 7.05-7.33 (m, 12H) 8.02 (br. s., 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08431702B2 |
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| Source dataset | uspto-grants-2013_04 |
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| ORD ID | ord-209ac2a01a8f4ea382c1b7a4fc35e256 |
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| Source note | uspto-grants-2013_04 |
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