HCID 59485920, compound → HCID 59485852, compound

Participants

Reaction Steps

The title compound is prepared as described in Example 276 from Example 290 and 2-fluorobenzonitrile. 1H NMR (CDCl3) δ 7.66 (dd, J=7.6, 1.6 Hz, 1H), 7.45-7.40 (m, 1H), 7.40-7.36 (m, 2H), 7.27-7.23 (m, 3H), 7.18-7.13 (m, 2H), 7.01-6.98 (m, 2H), 6.90-6.86 (m, 4H), 6.68 (dd, J=8.8, 0.8 Hz, 1H), 5.22 (dd, J=9.2, 6.8 Hz, 1H), 4.06 (t, J=9.2 Hz, 1H), 3.90-3.76 (m, 2H), 3.44-3.29 (m, 3H), 3.00 (s, 3H); HPLC-MS calculated for C31H26ClN3O5S (M+H+): 588.1, found 588.1.

Provenance & Evidence