HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1972288Generated: November 1, 2026
Tetrabutylammonium Fluoride → HCID 59485667, compound
https://huagongshe.com/reaction/1972288
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 86645373 | HCID 86645373 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59485667 | HCID 59485667 | — |
Reaction Steps
The crude product from step C is dissolved in anhydrous THF and tetrabutylammonium fluoride (67 uL) is added. The mixture is flushed with N2 and sealed in a microwave tube. The tube is put into a microwave reactor and heated to 100° C. for 5 min. The residue is purified by preparatory LC/MS to provide the title compound; HPLC-MS calculated for C26H27ClF3N4O2 (M+H+) 519.1, found 519.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08431607B2 |
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| Source dataset | uspto-grants-2013_04 |
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| ORD ID | ord-d1a5f259e4f44079b7444a7ecb934d61 |
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| Source note | uspto-grants-2013_04 |
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