1,1-Bis(methylthio)-2-nitroethylene → HCID 68707403, compound

Participants

Reaction Conditions

Reaction Steps

1,1-Bis(methylthio)-2-nitroethylene (13.1 mg, 0.079 mmol) and (S)—N1-(4-(4-chlorophenoxy)phenyl)-1-(3-(trifluoromethyl)phenyl)ethane-1,2-diamine prepared from Example 173 Step A (16.1 mg, 0.040 mmol) are dissolved in iPrOH (0.4 mL) and heated at 80° C. for 2 h. The solvent is removed and the residue is purified by preparatory LC/MS to provide the title compound; HPLC-MS calculated for C23H17ClF3N3O3 (M+H+) 476.1, found 476.1.

Provenance & Evidence