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2-Benzyl-6-bromo-2H-indazole → 2-Benzyl-6-chloro-5-fluoro-2H-indazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Benzyl-6-bromo-2H-indazole | HCID 58529689 | — |
| 反応物 | 6-chloro-5-fluoro-1H-indazole | HCID 58529904 | — |
| 生成物 | 2-Benzyl-6-chloro-5-fluoro-2H-indazole | HCID 58529592 | — |
反応手順
This compound was prepared in a manner similar to the procedure described for the preparation of 2-benzyl-6-bromo-2H-indazole, using 6-chloro-5-fluoro-1H-indazole in place of 6-bromoindazole. 1H-NMR (300 MHz, DMSO-d6) 8.54 (s, 1H), 7.90 (d, 1H), 7.71 (d, 1H), 7.36 to 7.29 (m, 5H), 5.64 (s, 2H); ES-MS m/z 261.0 [M+H]+, RT (min) 3.56.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08431695B2 |
| 出典データセット | uspto-grants-2013_04 |
| ORD ID | ord-08504bf612ff4d49958303b44747c49d |
| 出典メモ | uspto-grants-2013_04 |