HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-benzyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-Indazole → HCID 58529881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-benzyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-Indazole | HCID 58529313 | — |
| Reactant | HCID 58529853 | HCID 58529853 | — |
| Product | HCID 58529881 | HCID 58529881 | — |
Reaction Steps
Using the procedure described in step 4 of Example 80, the product from step 3 above and Intermediate C were converted to the title compound. 1H NMR (CD2Cl2) 1.50 (s, 9H), 1.60 (m, 1H), 1.80 (m, 2H), 2.80 (m, 3H), 4.10-4.30 (m, 3H), 5.60 (s, 2H), 5.80 (br, 2H), 7.00 (s, 1H), 7.10-7.50 (m, 9H), 7.80 (m, 2H), 7.90 (m, 2H), 7.95 (s, 1H), 8.10 (s, 1H); LC-MS [M+H]+=600.1, RT=3.55 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08431695B2 |
| Source dataset | uspto-grants-2013_04 |
| ORD ID | ord-ad0e48f5536543dfb2efc8ee6bf7a606 |
| Source note | uspto-grants-2013_04 |