Isopropylamine → HCID 637899, compound

HRID 1973081Notes

Reaction equation

HRID 1973081 reaction equation
[C:1]1(=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:8]([NH2:11])([CH3:10])[CH3:9]>>[CH3:9][CH:8]([N:11]=[C:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)[CH3:10]

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 7967Cyclohexanone

Product 1

HCID 637899HCID 637899, compound

Procedure

To a mixture of 600 g. cyclohexanone and 1 l. isopropylamine are added 500 g. Linde Type 3A molecular sieves. The mixture is allowed to stand overnight at room temperature, after which the excess isopropylamine is removed in vacuo at room temperature. The oily residue is 1-methyl-N-(cyclohexylidene)-ethylamine.

Workup

  1. additionTo a mixture of 600 g
  2. customafter which the excess isopropylamine is removed in vacuo at room temperature

Sources & evidence

ORD record
ord-be0c073cca6e4aeda9d221a3d9ea53a7
Source dataset
uspto-grants-1976_12
Patent number
US03996227

Reaction notes

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