HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Propynyl)piperazine → HCID 21492752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Propynyl)piperazine | HCID 14627369 | — |
| Reactant | 10-Chloro-8-fluoro-10,11-dihydro-3-methyldibenzo[b,f]thiepin | HCID 21416157 | — |
| Product | HCID 21492752 | HCID 21492752 | — |
Reaction Steps
In a manner analogous to that described in Example 1, from 10-chloro-10,11-dihydro-3-methyl-8-fluoro-dibenzo[b,f]thiepin and N-(2-propynyl)-piperazine there is obtained 1-[10,11-dihydro-3-methyl-8-fluoro-dibenzo[b,f]thiepin-10-yl]-4-(2-propynyl)-piperazine, the dimethanesulfonate of which melts at 168°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996229 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-53e152fb228b4aedaa27fb26c2c427e9 |
| Source note | uspto-grants-1976_12 |