Sodium Hydroxide → Sodium 2-(2,2,2-trifluoroethoxy)benzoate

HRID 1973195Notes

Reaction equation

HRID 1973195 reaction equation
[F:1][C:2]([F:15])([F:14])[CH2:3][O:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7]([OH:9])=[O:8].[OH-].[Na+:17]>C(O)C>[F:1][C:2]([F:14])([F:15])[CH2:3][O:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7]([O-:9])=[O:8].[Na+:17]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 115286442-(2,2,2-Trifluoroethoxy)benzoic acid

Product 1

HCID 23667245Sodium 2-(2,2,2-trifluoroethoxy)benzoate

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

2-(2,2,2-Trifluoroethoxy)benzoic acid is dissolved in ethanol and treated with an equimolar amount of sodium hydroxide dissolved in a minimum amount of ethanol and stirred for one hour. The solvent is removed by evaporation in vacuo to give sodium 2-(2,2,2-trifluoroethoxy)benzoate.

Workup

  1. customThe solvent is removed by evaporation in vacuo

Sources & evidence

ORD record
ord-97541fd137ba4d359a217ce8430a7afe
Source dataset
uspto-grants-1976_12
Patent number
US03996280

Reaction notes

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