HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-{3-Methyl-2-[nitro(phenylsulfanyl)methylidene]imidazolidin-1-yl}ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1-Methyl-2-[nitro(phenylsulfanyl)methylidene]imidazolidine | HCID 70639009 | — |
| Product | 1-{3-Methyl-2-[nitro(phenylsulfanyl)methylidene]imidazolidin-1-yl}ethan-1-one | HCID 54448094 | — |
Reaction Steps
20 ml of acetic anhydride and 1.26 g of 1B were heated together at 100° for 1 hour. The resulting mixture was cooled on an ice-bath and filtered to give 1, as a yellow crystals, m.p.: 191°-193° (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03996372 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-6e684842b18b46bfb374b92481e88660 |
| Source note | uspto-grants-1976_12 |