2-(4-bromobutyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione → HCID 131710565, compound

HRID 1973258Notes

Reaction equation

HRID 1973258 reaction equation
[ClH:1].[O:2]=[C:3]1[C:7]2([CH2:12][CH2:11][N:10]([CH2:13][CH2:14]CCN3C(=O)C4C=CC=C5C=4C(=CC=C5)C3=O)[CH2:9][CH2:8]2)[N:6]([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[CH2:5][NH:4]1.BrCC[CH2:41][CH2:42][CH2:43][N:44]1[C:53](=[O:54])[C:52]2[CH:55]=[CH:56][CH:57]=[C:50]3[C:51]=2[C:46](=[CH:47][CH:48]=[CH:49]3)[C:45]1=[O:58].BrCCCCN1C(=O)C2C=CC=C3C=2C(=CC=C3)C1=O>>[ClH:1].[O:2]=[C:3]1[C:7]2([CH2:8][CH2:9][N:10]([CH2:13][CH2:14][CH2:41][CH2:42][CH2:43][N:44]3[C:53](=[O:54])[C:52]4[CH:55]=[CH:56][CH:57]=[C:50]5[C:51]=4[C:46](=[CH:47][CH:48]=[CH:49]5)[C:45]3=[O:58])[CH2:11][CH2:12]2)[N:6]([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[CH2:5][NH:4]1

Participants

4

Reactant 3

HCID 27823602-(4-bromobutyl)-1H-benzo[de]isoquinoline-1,3(2H)-dioneHCID 166387912-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dioneHCID 131710564HCID 131710564, compound

Product 1

HCID 131710565HCID 131710565, compound

Procedure

Following the procedure of part (b) of example 26 but substituting 2-(5-bromopentyl)-1H-benz[de]isoquinoline-1,3(2H)-dione for the 2-(4-bromobutyl)-1H-benz[de]isoquinoline-1,3(2H)-dione, one obtains the titled compound.

Sources & evidence

ORD record
ord-b8716dbd93954add8f95ea4492f327e4
Source dataset
uspto-grants-1976_12
Patent number
US03996363

Reaction notes

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