1,4-Dibromobutane → 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione

HRID 1973259Notes

Reaction equation

HRID 1973259 reaction equation
Cl.O=C1C2(CCN([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:26](=[O:27])[C:25]4[CH:28]=[CH:29][CH:30]=[C:23]5[C:24]=4[C:19](=[CH:20][CH:21]=[CH:22]5)[C:18]3=[O:31])CC2)N(C2C=CC=CC=2)CN1.[Br:38][CH2:39][CH2:40]CCCCBr.BrCCCCBr>>[Br:38][CH2:39][CH2:40][CH2:13][CH2:14][CH2:15][CH2:16][N:17]1[C:26](=[O:27])[C:25]2[CH:28]=[CH:29][CH:30]=[C:23]3[C:24]=2[C:19](=[CH:20][CH:21]=[CH:22]3)[C:18]1=[O:31]

Participants

4

Reactant 3

HCID 80561,4-DibromobutaneHCID 123681,6-DibromohexaneHCID 131710564HCID 131710564, compound

Product 1

HCID 203645072-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione

Procedure

Following the procedure of part (a) of example 26 but substituting 1,6-dibromohexane for the 1,4-dibromobutane, one obtains 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione; m.p. 95°-96°.

Sources & evidence

ORD record
ord-e53037d0dc714b14a7b7b1959840eede
Source dataset
uspto-grants-1976_12
Patent number
US03996363

Reaction notes

Loading…