2-(4-bromobutyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione → HCID 131710566, compound

HRID 1973260Notes

Reaction equation

HRID 1973260 reaction equation
[ClH:1].[O:2]=[C:3]1[C:7]2([CH2:12][CH2:11][N:10](CCCCN3C(=O)C4C=CC=C5C=4C(=CC=C5)C3=O)[CH2:9][CH2:8]2)[N:6]([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[CH2:5][NH:4]1.Br[CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][N:45]1[C:54](=[O:55])[C:53]2[CH:56]=[CH:57][CH:58]=[C:51]3[C:52]=2[C:47](=[CH:48][CH:49]=[CH:50]3)[C:46]1=[O:59].BrCCCCN1C(=O)C2C=CC=C3C=2C(=CC=C3)C1=O>>[ClH:1].[O:2]=[C:3]1[C:7]2([CH2:8][CH2:9][N:10]([CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][N:45]3[C:54](=[O:55])[C:53]4[CH:56]=[CH:57][CH:58]=[C:51]5[C:52]=4[C:47](=[CH:48][CH:49]=[CH:50]5)[C:46]3=[O:59])[CH2:11][CH2:12]2)[N:6]([C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)[CH2:5][NH:4]1

Participants

4

Reactant 3

HCID 27823602-(4-bromobutyl)-1H-benzo[de]isoquinoline-1,3(2H)-dioneHCID 203645072-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dioneHCID 131710564HCID 131710564, compound

Product 1

HCID 131710566HCID 131710566, compound

Procedure

Following the procedure of part (b) of example 26 but substituting 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione for the 2-(4-bromobutyl)-1H-benz[de]isoquinoline-1,3-(2H)-dione, one obtains the titled compound.

Sources & evidence

ORD record
ord-eb2a236c38574d718ee53f55a775d163
Source dataset
uspto-grants-1976_12
Patent number
US03996363

Reaction notes

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