HRID1973326

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13203

2-Chlorocyclohexanone

C6H9ClO

HCID61217

1,2-Dimercaptopropane

C3H8S2

PRODUCTS

生成物

HCID12920049

2-Methyl-2,3,5,6,7,8-hexahydro-1,4-benzodithiine

C9H14S2

收率 66%

PROCEDURE

实验过程

The procedure of Example 1(a) is followed using 2-chloro-cyclohexanone and 1,2-propanedithiol to give 5,6,7,8-tetrahydro-2-methyl-1,4-benzodithian as a greenish oil, bp 127°-130°/2.3 mm, Yield 66%. NMR, 1.36 (3d), 1.4-1.88 (4m), 1.88-2.3 (4m), 2.6-3.7 (3m). IR, 2920, 1615, 1410, 1325, 1250, 1120, 855, 715.