HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → Aceclidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 14389216 | HCID 14389216 | — |
| Product | Aceclidine | HCID 1979 | — |
Reaction Steps
The thus obtained (+) quinuclidinol was esterified with acetic anhydride to yield in a quantitative manner the desired novel (+) 3-acetoxy quinuclidine. The hydrochloride was obtained from a solution of hydrogen chloride in anhydrous ether, M.P. = 175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997543 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-20480790eb40449ebe2f0f529fbf68f1 |
| Source note | uspto-grants-1976_12 |