HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Chloroanilino)quinolizin-5-ium bromide → HCID 12446537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Chloroanilino)quinolizin-5-ium bromide | HCID 12446527 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 12446537 | HCID 12446537 | — |
Reaction Steps
A suspension of 2-(4-chloroanilino)quinolizinium bromide (30 g., 0.09 mole) in 500 ml of 1N NaOH solution was warmed to 50° and stirred for 30 minutes. The crude product was removed by filtration and dried. The product (20 g., 87%) was recrystallized from ethanol to give material which melted at 183°-184°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997547 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-f401ada7aa924e868d07d4af5354a9d0 |
| Source note | uspto-grants-1976_12 |