HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → Carbendazim
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Methyl N-cyanocarbamate | HCID 89023 | — |
| Product | Carbendazim | HCID 25429 | 94% |
Reaction Steps
The salt of methyl cyanocarbamate with o-phenylenediamine (1.0 parts) is heated at 145°-50° C. for 10 minutes. This treatment gives 0.86 parts (94% yield) of 2-benzimidazolecarbamic acid, methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03997553 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-16f34176f1404291970f6ca3cb56cabf |
| Source note | uspto-grants-1976_12 |