HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dichloroanthraquinone → HCID 21489835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dichloroanthraquinone | HCID 6711 | — |
| Reactant | 2,5-Dichloroaniline | HCID 7262 | — |
| Catalyst | Copper | HCID 23978 | — |
| Product | HCID 21489835 | HCID 21489835 | — |
Reaction Steps
If, analogously to the above example, 2,5-dichloroaniline is condensed with 1,5-dichloroanthraquinone in the presence of a mixture of 0.5 part of copper powder and 0.5 part of copper-I chloride as the catalyst, instead of the copper-I iodide/picoline complex, only 12 parts of 1,5-bis-(2,5-dichloroanilino)anthraquinone are obtained, corresponding to a yield of only 23%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998780 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-4c89703cfee445fc9138ee966f5973ca |
| Source note | uspto-grants-1976_12 |