Ethanethiol → HCID 21490449, compound

HRID 1973713Notes

Reaction equation

HRID 1973713 reaction equation
[CH2:1]([N:4]=[C:5]=[O:6])[CH:2]=[CH2:3].[CH2:7]([SH:9])[CH3:8]>>[CH2:7]([S:9][CH2:3][CH2:2][CH2:1][N:4]=[C:5]=[O:6])[CH3:8]

Participants

3

Reactant 2

HCID 6343EthanethiolHCID 15123Allyl isocyanate

Product 1

HCID 21490449HCID 21490449, compound

Procedure

A mixture of 16.6 grams (0.2 mole) of allyl isocyanate and 12.4 grams (0.2 mole) of ethanethiol is irradiated at -30° C for 24 hours in the manner described in Example 1 to yield the olefinic adduct, i.e. 3-ethylthiopropyl isocyanate as the major product.

Workup

  1. customis irradiated at -30° C for 24 hours in the manner

Sources & evidence

ORD record
ord-462dbe918a2448ae8d2586531ddfdffc
Source dataset
uspto-grants-1976_12
Patent number
US03998866

Reaction notes

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