p-Toluenesulfonyl isocyanate → HCID 20325614, compound

HRID 1973749Notes

Reaction equation

HRID 1973749 reaction equation
[CH3:1][CH:2]1[CH2:7][C:6](=[O:8])[CH2:5][C:4](=[O:9])[CH2:3]1.[C:10]1([CH3:22])[CH:15]=[CH:14][C:13]([S:16]([N:19]=[C:20]=[O:21])(=[O:18])=[O:17])=[CH:12][CH:11]=1>C1C=CC=CC=1>[CH3:1][CH:2]1[CH2:7][C:6](=[O:8])[CH:5]([C:20](=[O:21])[NH:19][S:16]([C:13]2[CH:14]=[CH:15][C:10]([CH3:22])=[CH:11][CH:12]=2)(=[O:17])=[O:18])[C:4](=[O:9])[CH2:3]1

Participants

4

Reactant 2

HCID 77703p-Toluenesulfonyl isocyanateHCID 4580955-Methylcyclohexane-1,3-dione

Product 1

HCID 20325614HCID 20325614, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Reaction of equimolar amounts of 5-methyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5 -METHYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 121.5°-122.5° C. (corr.).

Sources & evidence

ORD record
ord-cd6066d9a3bf4de18419d25537921812
Source dataset
uspto-grants-1976_12
Patent number
US03998879

Reaction notes

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