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HRID1973753

反应详情

EQUATION

反应方程式

HRID 1973753 的结构方程式

REACTANTS

反应物

2
反应SMILES：Cc1ccc(S(=O)(=O)N=C=O)cc1
HCID77703

p-Toluenesulphonyl isocyanate

C8H7NO3S

反应SMILES：O=C1CC(=O)CC2(CCCCC2)C1
HCID4962152

spiro[5.5]undecane-2,4-dione

C11H16O2

PRODUCTS

产物

1
反应SMILES：Cc1ccc(S(=O)(=O)NC(=O)C2C(=O)CC3(CCCCC3)CC2=O)cc1
HCID328866

NSC309741

C19H23NO5S

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

Reaction of equimolar amounts of spiro[5.5]undecane-2,4-dione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 3-[N-(p-TOLUENESULFONYL)CARBAMOYL]SPIRO-[5.5]UNDECANE-2,4-DIONE, m.p. 150.5°-152° C. (corr.).