Dimedone → HCID 20325603, compound

HRID 1973754Notes

Reaction equation

HRID 1973754 reaction equation
[CH3:1][C:2]1([CH3:10])[CH2:7][C:6](=[O:8])[CH2:5][C:4](=[O:9])[CH2:3]1.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([S:18]([N:21]=[C:22]=[O:23])(=[O:20])=[O:19])=[CH:14][CH:13]=1>C1C=CC=CC=1>[Cl:11][C:12]1[CH:13]=[CH:14][C:15]([S:18]([NH:21][C:22]([CH:5]2[C:6](=[O:8])[CH2:7][C:2]([CH3:10])([CH3:1])[CH2:3][C:4]2=[O:9])=[O:23])(=[O:19])=[O:20])=[CH:16][CH:17]=1

Participants

4

Reactant 2

HCID 31358DimedoneHCID 1385874-Chlorobenzenesulfonyl isocyanate

Product 1

HCID 20325603HCID 20325603, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Reaction of equimolar amounts of 5,5-dimethylcyclohexane-1,3-dione with p-chlorobenzenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 2-(N-p-CHLOROBENZENESULFONYLCARBAMOYL)-5,5-DIMETHYLCYCLOHEXANE-1,3-DIONE, m.p. 103°-105.5° C. (corr.).

Sources & evidence

ORD record
ord-2af81335f4064850a3248cdc72052d0c
Source dataset
uspto-grants-1976_12
Patent number
US03998879

Reaction notes

Loading…