huagongshe.com
HRID1973755

反应详情

EQUATION

反应方程式

HRID 1973755 的结构方程式

REACTANTS

反应物

2
结构：O=C=NS(=O)(=O)c1ccc(Cl)cc1
HCID138587

p-Chlorobenzenesulfonyl isocyanate

C7H4ClNO3S

结构：CC(C)C1CC(=O)CC(=O)C1
HCID566106

5-Isopropyl-1,3-cyclohexanedione

C9H14O2

PRODUCTS

生成物

1
结构：CC(C)C1CC(=O)C(C(=O)NS(=O)(=O)c2ccc(Cl)cc2)C(=O)C1
HCID20325613

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

Reaction of equimolar amounts of 5-isopropyl-1,3-cyclohexanedione with p-chlorobenzenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 2-(N-p-CHLOROBENZENESULFONYLCARBAMOYL)-5-ISOPROPYL-1,3-CYCLOHEXANEDIONE, m.p. 100.5°-101.5° C. (resolidified and melting at 183.5° C. with dec.)(corr.).