HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimedone → N-(Benzenesulfonyl)-4,4-dimethyl-2,6-dioxocyclohexane-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimedone | HCID 31358 | — |
| Reactant | Phenylsulphonyl isocyanate | HCID 76096 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N-(Benzenesulfonyl)-4,4-dimethyl-2,6-dioxocyclohexane-1-carboxamide | HCID 20325619 | — |
Reaction Steps
Reaction of equimolar amounts of 5,5-dimethyl-1,3-cyclohexanedione with benzenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5,5-DIMETHYL-2-(N-BENZENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 101°-103° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-c991e1f75ce84779800afc65a7db72bd |
| Source note | uspto-grants-1976_12 |