p-Toluenesulfonyl isocyanate → HCID 20325612, compound

HRID 1973757Notes

Reaction equation

HRID 1973757 reaction equation
[CH2:1]([CH:3]([CH:6]1[CH2:11][C:10](=[O:12])[CH2:9][C:8](=[O:13])[CH2:7]1)[CH2:4][CH3:5])[CH3:2].[C:14]1([CH3:26])[CH:19]=[CH:18][C:17]([S:20]([N:23]=[C:24]=[O:25])(=[O:22])=[O:21])=[CH:16][CH:15]=1>C1C=CC=CC=1>[CH2:1]([CH:3]([CH:6]1[CH2:7][C:8](=[O:13])[CH:9]([C:24](=[O:25])[NH:23][S:20]([C:17]2[CH:18]=[CH:19][C:14]([CH3:26])=[CH:15][CH:16]=2)(=[O:21])=[O:22])[C:10](=[O:12])[CH2:11]1)[CH2:4][CH3:5])[CH3:2]

Participants

4

Reactant 2

HCID 77703p-Toluenesulfonyl isocyanateHCID 203256185-(Pentan-3-yl)cyclohexane-1,3-dione

Product 1

HCID 20325612HCID 20325612, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Reaction of equimolar amounts of 5-(1-ethylpropyl)-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-(1-ETHYLPROPYL)-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 111.5°-112.5° C. (corr.).

Sources & evidence

ORD record
ord-cc3458e86c6147b79b4e0c0d2121ea54
Source dataset
uspto-grants-1976_12
Patent number
US03998879

Reaction notes

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