HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylacetone → HCID 20325620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylacetone | HCID 7166 | — |
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20325620 | HCID 20325620 | — |
Reaction Steps
Reaction of equimolar amounts of 1-phenyl-1,3-butanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 1-PHENYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-BUTANEDIONE, m.p. 113.5°-116.5° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-786e337e01bd44bf878c1d581cf66039 |
| Source note | uspto-grants-1976_12 |