HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonyl isocyanate → 5-PROPYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Reactant | 5-Propylcyclohexane-1,3-dione | HCID 2737224 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-PROPYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE | HCID 20325606 | — |
Reaction Steps
Reaction of equimolar amounts of 5-propyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-PROPYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 132.5°-133.5° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-0cc881c85c22499c987092b7f1a4bb9e |
| Source note | uspto-grants-1976_12 |