HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylsulphonyl isocyanate → 4-(1-Methylethyl)-2,6-dioxo-N-(phenylsulfonyl)cyclohexanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylsulphonyl isocyanate | HCID 76096 | — |
| Reactant | 5-(Isopropyl)cyclohexane-1,3-dione | HCID 566106 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-(1-Methylethyl)-2,6-dioxo-N-(phenylsulfonyl)cyclohexanecarboxamide | HCID 20325609 | — |
Reaction Steps
Reaction of equimolar amounts of 5-isopropyl-1,3-cyclohexanedione with benzenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-ISOPROPYL-2-(N-BENZENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 112.5°-114° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-fca5d0e0a4c74e08b26ab5cf8cf099a8 |
| Source note | uspto-grants-1976_12 |