HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Pentanedione, 1-phenyl- → HCID 20325604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Pentanedione, 1-phenyl- | HCID 18723 | — |
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20325604 | HCID 20325604 | — |
Reaction Steps
Reaction of equimolar amounts of 1-phenyl-2,4-pentanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 1-PHENYL-3-(N-p-TOLUENESULFONYLCARBAMOYL)-2,4-PENTANEDIONE, m.p. 119.5°-120.5° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-3e4b8f1f8964414398e21b819b7f42c8 |
| Source note | uspto-grants-1976_12 |